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Beilstein J. Org. Chem. 2014, 10, 2131–2138, doi:10.3762/bjoc.10.220
Graphical Abstract
Figure 1: A constitutional and conformational (idealized) representation of isoGNA, an isomer of glycerol nuc...
Scheme 1: Initial routes towards the synthesis of iso-glycerol nucleosides.
Scheme 2: Preparation of thymine and adenine containing phosphoramidites of isoGNA.
Scheme 3: Preparation of guanine- and cytosine-containing phosphoramidites of isoGNA.
Scheme 4: Preparation of adenine containing phosphoramidite of isoGNA.
Scheme 5: Mitsunobu reaction with the di-Boc-adenine.
Scheme 6: An attempt to remove both Boc and silyl groups simultaneously.
Scheme 7: The synthesis of 26 via tritylation and benzoylation.